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Saturday, May 2, 2020 | History

3 edition of Solid-State Nmr Techniques found in the catalog.

Solid-State Nmr Techniques

Jacek Klinowski

Solid-State Nmr Techniques

  • 181 Want to read
  • 34 Currently reading

Published by Imperial College Press .
Written in English

    Subjects:
  • Chemical spectroscopy, spectrochemistry,
  • Physical chemistry,
  • Solid State Chemistry,
  • Nmr Spectroscopy In Chemistry,
  • Science,
  • Science/Mathematics,
  • Chemistry - Physical & Theoretical

  • The Physical Object
    FormatHardcover
    Number of Pages200
    ID Numbers
    Open LibraryOL12055565M
    ISBN 101860940897
    ISBN 109781860940897

      Solid State NMR Spectroscopy by Melinda J. Duer, , available at Book Depository with free delivery : Melinda J. Duer. Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques.


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Solid-State Nmr Techniques by Jacek Klinowski Download PDF EPUB FB2

The book provides Solid-State Nmr Techniques book engineers, analytical chemists, and physicists, in and out of laboratories, a survey of the techniques and the essential tools of solid-state NMR, together with a 5/5(1). NMR Theory. This section is intended to Solid-State Nmr Techniques book an overview of solid state NMR for someone unfamiliar with NMR techniques.

For a more comprehensive theoretical explanation of NMR we recommend a few web resources on NMR and EPR which can be particularly useful due to their conciseness and clarity. Introduction to Solid State NMR Spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid-state nuclear magnetic resonance spectroscopy or undertaking research projects where solid-state NMR is likely to be a major investigative technique.

It will also serve as a practical introduction in industry, where the techniques can provide Cited by: About this book. Solid-state NMR covers an enormous range of material types and experimental techniques. Although the basic instrumentation and techniques of solids NMR are readily accessible, there can be significant barriers, even for existing experts, to exploring the bewildering array of more sophisticated techniques.

This book provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these techniques in heterogeneous catalysts and related catalytic reactions, which is suitable as a reference guide for both experienced researchers in and newcomers.

Solid-State NMR IV, Methods and Applications of Solid-State NMR in NMR Basic Principles and Progress, Vol. 33 Bernhard Blümich (Ed.), Springer-Verlag, Berlin ().

Multidimensional Solid-State NMR and Polymers, Klaus Schmidt-Rohr and Hans Wolfgang Spiess, Academic, London (). Nuclear Magnetic Resonance Probes of Molecular Dynamics. Many solid-state NMR techniques mimic the free tumbling of molecules in liquids by spinning the sample during data acquisition.

Spinning rapidly enough at a specific angle to the baseline magnetic field – the magic angle – can narrow spectral lines, boosting resolution. Introduction to Solid State NMR Spectroscopy is written for undergraduate and graduate students of chemistry, either taking a course in advanced or solid-state nuclear magnetic resonance spectroscopy or undertaking research projects where solid-state NMR is likely to be a major investigative technique.

It will also serve as a practical introduction in industry, where the techniques can provide Author: Melinda J. Duer. The book provides an in-depth review of the state of the art of NMR spectroscopy as applied to a wide range of geochemical problems. It is intended to assist geochemists and spectroscopists working at the interface between geochemistry and NMR, and almost all areas of organic and inorganic geochemistry where NMR has had an influence are discussed.

The nuclear magnetic resonance (NMR) spectroscopy is a very powerful tool in the chemical characterization, both in solution and in solid state. With the development of NMR spectrometers more potent field, employing radio frequency pulse, provided the development of studies on materials, especially amorphous materials.

Thus, there was a need to develop techniques to obtain spectra in Author: Maria Ines Bruno Tavares. Additionally, it is non-destructive, which can allow the same sample to be re-analyzed using other techniques. How we can use solid-state NMR.

Solid-state NMR spectra of pharmaceutical solids are primarily acquired using magic-angle spinning with cross-polarization, most often with 13 C detection. The method has been applied in a number of.

This book is for those familiar with solution-state NMR who are encountering solid-state NMR for the first time. It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details.

This dual requirement is met through careful construction of 4/5(1). The book is divided into two parts: "Fundamentals" and "Further Applications." The section on Fundamentals contains relatively long chapters that deal with the basic theory and practice of solid-state NMR.

The essential differences and extra scope of solid-state NMR over solution-state is dealt with in an introductory chapter. Solid-state NMR (ssNMR) spectroscopy is a special type of nuclear magnetic resonance (NMR) spectroscopy, characterized by the presence of anisotropic (directionally dependent) interactions.

Compared to the more common solution NMR spectroscopy, ssNMR usually requires additional hardware for high-power radio-frequency irradiation and magic-angle spinning. Photis Dais, Apostolos Spyros, in Chemical Analysis of Food: Techniques and Applications, High-Resolution Solid-State NMR Spectroscopy.

Solid-state NMR spectra of protons cannot be recorded with the technology described for dilute spins, owing to the presence of strong homonuclear dipolar couplings among the 1 H spins.

Exception to this unfortunate situation may be the semi-solid. Basic Theory of the Solid‐state NMR Techniques. Solid‐state NMR Studies of the Structure. Conformation and Conversion of Molecules Adsorbed in Porous Materials.

Pulsed Field Gradient (PFG) NMR Technique. Magnetic Resonance Imaging of Porous Materials. X e NMR Conclusions. Symbols and Abbreviations. Dipolar Recoupling, by Niels Chr. Nielsen, Lasse A. Strassø and Anders B. Nielsen.-Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C.

Chan.-Solid-State 19F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch. Solid-State NMR Techniques for the Structural Determination of Amyloid Fibrils, by Jerry C.

Chan.-Solid-State 19 F-NMR of Peptides in Native Membranes, by Katja Koch, Sergii Afonin, Marco Ieronimo, Marina Berditsch and Anne S. Ulrich Modern solid-state NMR is now employed across a wide range of fields including solid-state physics in semiconductors, materials science and engineering, and study of large biomolecules.

Current Work Current work in our lab involves the application of solid state NMR techniques and theories to s olid state polarization and detection, NV spin. Hence solid-state NMR is a field in itself, separate from solution-state NMR, and is generally considered more difficult.

Which is why it is not as routine as solution state nmr. Introduction to Solid State NMR In solution NMR, spectra consist of a series of very sharp transitions, due to averaging of anisotropic NMR interactions by rapid random tumbling. By contrast, solid-state NMR spectra are very broad, as the full effects of anisotropic or orientation-dependent interactions are observed in the spectrum.

The NOOK Book (eBook) of the Solid State NMR of Polymers by T. Asakura at Barnes & Noble. FREE Shipping on $35 or more. Due to COVID, orders may be delayed. Thank you for your patience. Book Annex Membership Educators Gift Cards Stores & Events Help Auto Suggestions are available once you type at least 3 letters.

Pages: Dipolar Solid State NMR Approaches Towards Medium-Range Structure in Oxide Glasses Hellmut Eckert, Stefan Elbers, Jan Dirk Epping, Michael Janssen, Martin Kalwei, Wenzel Strojek et. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR.

Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better 4/5(1). Request PDF | Solid-State NMR Principles and Techniques | This chapter gives a brief introduction of nuclear spin interactions in solids.

Then techniques to manipulate these internal interactions. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better.

Nuclear magnetic resonance (NMR) spectroscopy is a powerful tool for characterization of materials. It can detect local structure around selected atomic nuclei and provide information on the dynamics of these nuclei.

In case of metal-organic frameworks, NMR spectroscopy can help elucidate the framework structure, locate the molecules adsorbed into the pores, and inspect and characterize the Cited by: 2. Filling a void in the current literature, NMR Spectroscopy of Biological Solids examines all the recent developments, implementation, and interpretation of solid-state NMR experiments and the advantages of applying them to biological systems.

The book emphasizes how these techniques can be used to realize the structure of non-crystalline. The journal Solid State Nuclear Magnetic Resonance publishes original manuscripts of high scientific quality dealing with all experimental and theoretical aspects of solid state NMR.

This includes advances in instrumentation, development of new experimental techniques and methodology, new theoretical insights, new data processing and simulation.

ISBN: OCLC Number: Description: 1 online resource (viii, pages): illustrations: Contents: Magic-angle spinning: A historical perspective / J. Hennel and J. Klinowski --New horizons for magic-angle spinning NMR / A.

Samoson [and others] --Strategies for high-resolution proton spectroscopy in solid-state NMR / E. Vinogradov, P. Madhu and S. Vega --High. Genre/Form: Electronic books: Additional Physical Format: Print version: New techniques in solid-state NMR.

Berlin ; New York: Springer, © (DNLM)nlb It includes an introduction to the basic theory of solid-state NMR and various frequently used techniques. Special emphasis is placed on characterizing the framework and pore structure, active site, guest-host interaction, and synthesis mechanisms of heterogeneous catalysts using multinuclear one- and two-dimensional solid-sate NMR spectroscopy.

Solid state NMR is a powerful, but subtle, technique for the characterisation of solid materials. It is strongly complementary to diffraction-based techniques (which are sensitive to long-range ordering) in that it probes local chemical environments and so can be applied successfully to all manner of materials whether crystalline or not, homogeneous or not.

Solid-state NMR is a powerful physical method widely applied in modern fundamental and applied science, medicine, and industry. Its role is particularly valuable in materials chemistry due to the capability of solid-state NMR to rapidly solve tasks connected with structural descriptions of complex systems on macro and/or molecular levels, and the identification of the dynamics often.

High-resolution solid-state NMR has recently been extensively applied to study structure and solid-state reactions of inorganic silicates, aluminosilicates and, in particular, zeolites.

In addition, a variety of NMR methods including conventional FT NMR techniques have been successfully used to investigate sorbate-sorbent interactions and the. Solid-state NMR Spectroscopy - An Introduction Rene Verel [email protected] HCI D Outline General Principles of NMR Spectroscopy Interactions relevant to NMR Spectroscopy (and their information content) Differences between solution and solid state NMR File Size: 1MB.

of solid state NMR probes. Several families of Magic Angle Spinning (MAS) probes, with sample diameters from to 7 mm, provide complete access to a comprehensive range of solid state NMR applications. While static probes are solely used for special applications, MAS is the routine method of choice, as it introduces resolution into the File Size: KB.

Summary. Solid-state NMR is a powerful physical method widely applied in modern fundamental and applied science, medicine, and industry. Its role is particularly valuable in materials chemistry due to the capability of solid-state NMR to rapidly solve tasks connected with structural descriptions of complex systems on macro and/or molecular levels, and the identification of the dynamics often.

@article{osti_, title = {High-resolution solid-state NMR of silicates and zeolites}, author = {Engelhardt, G and Michel, D}, abstractNote = {Although the basic principles and methods of high-resolution solid-state NMR are presented in this volume, the emphasis is on applications.

References are extensive and include material published in. Nuclear magnetic resonance spectroscopy, most commonly known as NMR spectroscopy or magnetic resonance spectroscopy (MRS), is a spectroscopic technique to observe local magnetic fields around atomic sample is placed in a magnetic field and the NMR signal is produced by excitation of the nuclei sample with radio waves into nuclear magnetic resonance, which is detected with sensitive.

Book Summary: The title of this book is Modern Methods in Solid-state NMR and it was written by Paul Hodgkinson (Editor), William S Price (Editor), Yusuke Nishiyama (Contributor).

This particular edition is in a Hardcover format. This books publish date is and it has a suggested retail price of $Book Edition: 1st.This book strikes a balance between state-of-the-art solid-state NMR techniques and the applications of these techniques to problems in materials science.

The applications focus on modern inorganic materials such as metal oxides, catalysts, zeolites, glasses, ceramics, semiconductors, ion conductors, superconductors, and composites.

The book features chapters on multiple-quantum MAS NMR. This book is for those familiar with solution-state benchtop NMR who are encountering solid-state NMR for the first time.

It presents the current understanding and applications of solid-state NMR with a rigorous but readable approach, making it easy for someone who merely wishes to gain an overall impression of the subject without details.